Please use this identifier to cite or link to this item: https://hdl.handle.net/20.500.12104/43022
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dc.contributor.authorUlloa-Godinez, S.
dc.contributor.authorBarrera, A.
dc.contributor.authorRosales, I.
dc.contributor.authorBucio, L.
dc.contributor.authorCastillon, F.F.
dc.contributor.authorFarias, M.H.
dc.contributor.authorSiqueiros, J.M.
dc.contributor.authorCampa-Molina, J.
dc.date.accessioned2015-09-15T18:27:43Z-
dc.date.available2015-09-15T18:27:43Z-
dc.date.issued2011
dc.identifier.urihttp://www.scopus.com/inward/record.url?eid=2-s2.0-84861116438&partnerID=40&md5=9bd28e529b2aa9d69bf29f0dde8ba4a2
dc.identifier.urihttp://ovidsp.ovid.com/ovidweb.cgi?T=JS&CSC=Y&NEWS=N&PAGE=fulltext&D=prem&AN=21770219
dc.identifier.urihttp://hdl.handle.net/20.500.12104/43022-
dc.description.abstractNew iron-zinc chlorine single crystals of Fe 1.5Zn 1.5B 7O 13Cl boracite were grown by chemical transport reactions in closed quartz ampoules, at a temperature of 1173 K. The crystal structure was characterized by X-ray powder diffraction (XRD) using the Rietveld refinement method and belongs to the trigonal/rombohedral system with space group R3c (No. 161). The cell parameters were a = 8.5726(1) �, c = 21.0116(4) �, V = 1337.26(3) � 3 and Z = 6. The refinement successfully proceeded and ended with sound merit figure values X 2 = 2.25, R B = 6.12%. Chemical analysis was performed with X-ray energy dispersive spectroscopy (EDS) and X-ray fluorescence (XRF). Ferroelectric nano and micro reoriented domains were found in this material using polarizing optical microscopy (PLM), scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The examination by TEM showed that in the trigonal/rombohedral system of Fe 1.5Zn 1.5B 7O 13Cl nanodomain structures exist. Thin (50-100 nm) mostly planar domains parallel to (100) were frequently observed in Fe 1.5Zn 1.5B 7O 13Cl boracite. Copyright � 2011 American Scientific Publishers.
dc.relation.isreferencedbyScopus
dc.relation.isreferencedbyMEDLINE
dc.relation.isreferencedbyWOS
dc.titleNano and micro reoriented domains and their relation with the crystal structure in the new Fe 1.5Zn 1.5B 7O 13Cl boracite
dc.typeConference Paper
dc.identifier.doi10.1166/jnn.2011.3438
dc.relation.ispartofjournalJournal of Nanoscience and Nanotechnology
dc.relation.ispartofvolume11
dc.relation.ispartofissue6
dc.relation.ispartofpage5562
dc.relation.ispartofpage5568
dc.subject.keywordDomain structure; New boracite; Structural characterization
dc.contributor.affiliationUlloa-God�nez, S., Centro Universitario de Ciencias Exactas e Ingenier�a, Universidad de Guadalajara, Departamento de Electr�nica, Av. Revoluci�n No.1500, Planta baja, S.R. C.P. 44840, Guadalajara, Jalisco, Mexico, Facultad de Ingenier�a, Universidad Aut�noma de Baja California, Blvd. Benito Juarez s/n col. Insurgentes, Mexicali, Baja California, Mexico; Barrera, A., Centro Universitario de la Ci�nega, Universidad de Guadalajara, Laboratorio de Materiales, Av. Universidad No. 1115, Colonia Linda Vista, C.P. 47840, Ocotl�n, Jalisco, Mexico; Rosales, I., Instituto de F�sica, Universidad Nacional Aut�noma de M�xico, Apartado Postal 20-364, C.P. 01000 M�xico, D. F., Mexico; Bucio, L., Instituto de F�sica, Universidad Nacional Aut�noma de M�xico, Apartado Postal 20-364, C.P. 01000 M�xico, D. F., Mexico; Castillon, F.F., Centro de Nanociencias y Nanotecnolog�a, Universidad Nacional Aut�noma de M�xico, Apdo. Postal 356, C.P. 22800, Ensenada, Baja California, Mexico; Farias, M.H., Centro de Nanociencias y Nanotecnolog�a, Universidad Nacional Aut�noma de M�xico, Apdo. Postal 356, C.P. 22800, Ensenada, Baja California, Mexico; Siqueiros, J.M., Centro de Nanociencias y Nanotecnolog�a, Universidad Nacional Aut�noma de M�xico, Apdo. Postal 356, C.P. 22800, Ensenada, Baja California, Mexico; Campa-Molina, J., Centro Universitario de Ciencias Exactas e Ingenier�a, Universidad de Guadalajara, Departamento de Electr�nica, Av. Revoluci�n No.1500, Planta baja, S.R. C.P. 44840, Guadalajara, Jalisco, Mexico
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